GROWTH AND CHARACTERIZATION OF NbSe2 SINGLE CRYSTALS VIA A SIMPLE CALCINATION PROCESS
نویسندگان
چکیده
The NbSe2 nanoplates with novel hexagonal morphology have been obtained via solid-state assembly of NbSe2 ultrathin nanosheets, which were prepared by a simple calcination process using micro-sized Nb and Se powders as the precursors. The influence of high-temperature annealing upon morphology of single-crystal NbSe2 was investigated. On the basis of experimental results of different temperatures and time-dependent morphology evolution process, a possible reaction process and a growth mechanism were preliminarily proposed.
منابع مشابه
INVESTIGATION ON GROWTH AND CHARACTERIZATION OF NONLINEAR OPTICAL DICHLORO-DIGLYCINE ZINC II SINGLE CRYSTAL
The study of amino acid based nonlinear optical (NLO) materials with optimum physical properties is an important area due to their practical applications such as optical communication, optical computing, optical information processing, optical disk data storage, laser fusion reactions, laser remote sensing, colour display, medical diagnostics, etc. Also, microelectronic industries require cryst...
متن کاملCharacterization and Investigation of Grain Selection in Spiral Grain Selectors during Casting Single-Crystal Turbine Blades
Manufactured single crystal components using Ni-base super alloys are routinely used in the hot sections of aero engines and industrial gas turbines due to their outstanding high temperature strength, toughness and resistance to degradation in corrosive and oxidative environments. To control the quality of the single crystal turbine blades, particular attention has been paid to grain selection,...
متن کاملCharacterization and Investigation of Grain Selection in Spiral Grain Selectors during Casting Single-Crystal Turbine Blades
Manufactured single crystal components using Ni-base super alloys are routinely used in the hot sections of aero engines and industrial gas turbines due to their outstanding high temperature strength, toughness and resistance to degradation in corrosive and oxidative environments. To control the quality of the single crystal turbine blades, particular attention has been paid to grain selection,...
متن کاملA simple and safe method for preparation of Mg(OH)2 nanorods in ambient air
Magnesium hydroxide Mg(OH)2 nanorods with diameters of 90±10nm and lengths of more than 2μms were prepared by a simple route at ~75oC in ambient air. The approach is based on reaction of magnesium powder and de-ionized water without the use of any harmful, toxic or corrosive reagents. Characterization using X-ray diffraction (XRD) shows single crystalline structure of Mg(O...
متن کاملA simple and safe method for preparation of Mg(OH)2 nanorods in ambient air
Magnesium hydroxide Mg(OH)2 nanorods with diameters of 90±10nm and lengths of more than 2μms were prepared by a simple route at ~75oC in ambient air. The approach is based on reaction of magnesium powder and de-ionized water without the use of any harmful, toxic or corrosive reagents. Characterization using X-ray diffraction (XRD) shows single crystalline structure of Mg(O...
متن کامل